By G.A. Webb (Ed.)
Content material: 1. Advances in Probe layout for Protein NMR. 2. Diffusion in smooth Polymer platforms as Approached by means of box Gradient NMR. three. How a ways Can the Sensitivity of NMR be elevated? four. functions of Low-Field NMR to nutrients technology. five. Residual Dipolar Couplings: Measurements and functions to Biomolecular stories
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Additional info for Annual Reports on NMR Spectroscopy, Vol. 58
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The largest S/N advantages occur at low magnetic fields or for small coils, both cases in which coil losses tend to dominate. ADVANCES IN PROBE DESIGN FOR PROTEIN NMR 25 Fig. 17. Sensitivity-enhanced 1H/15N HSQC spectra acquired in 10 min on a 50 mM sample of the catalytic domain of stromelysin using (A) a dual (15N/1H) inverse Cryoprobe (Bruker) equipped with a lock and a z-gradient and (B) a conventional triple-resonance (13C/15N/1H) inverse probe (Nalorac). 4 was realized with the Cryoprobe as compared to the conventional TXI probe.